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Table 1 Chemical shift assignments for 1H-NMR and 13C-NMR spectra of agaro-oligosaccharides

From: Antioxidant activity and hepatoprotective potential of agaro-oligosaccharides in vitro and in vivo

Unit

Chemical shifts (ppm)

  

C-1

C-2

C-3

C-4

C-5

C-6

Carbon

G a

102.3

70.6

82.3

68.7

75.2

61.2

 

A b

98.1

69.9

79.7

77.1

75.5

69.4

Proton

G

4.39

3.79

3.6

4.12

3.55

3.63 c/3.67 d

 

A

4.97

3.96

4.37

4.48

4.4

3.84 e/4.06 f

  1. a galactose.
  2. b anhydrogalactose.
  3. c A-6 exo proton
  4. d A-6'endo proton
  5. e G-6 proton
  6. f G-6' proton